Journal of the Graduate School of Biosphere Science, Hiroshima University Volume 45
2006-12-20 発行

沿岸域における生物起源ケイ素の分析手法の検討と春季周防灘における分布

Evaluation for the Measurement of Biogenic Silicon in Coastal Waters and the Distribution in Suspended Matters of Suo-nada, Seto Inland Sea
Nakajima, Sayaka
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abstract
Measurement of biogenic silicon (BSi) in suspended matter and sediments is not simple because of the interference of lithogenic silicon (LSi) in the samples, particularly in coastal waters. We tested applicability and limits of a wet-alkaline digestion method for BSi analysis in suspended matter and sediments collected at Suo-nada, Seto Inland Sea.

For suspended matter, a digestion (using 1%Na2CO3) at 85 ℃ for 60 min was appropriate, and digestion for 120-180 min was suitable for sediments. We also tested the interference of alkaline solution to the Si analysis using by the molybdenum blue method. Dilution factor more than 5 times by MQ water or neutralizing the pH by 0.5N HCl was recommended for the method. By applying this method, a preliminary investigation on BSi in suspended matter at Suo-nada was conducted in April 2004.
subject
アルカリ抽出法, 周防灘, 生物起源ケイ素(BSi)
wet-alkaline digestion
Suo-nada
biogenic silicon (BSi)
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